نوع مقاله : مقاله کامل پژوهشی

نویسندگان

1 کارشناسی ارشد، دانشکده فنی و مهندسی، واحد شاهرود، دانشگاه آزاد اسلامی، شاهرود، سمنان، ایران

2 استاد، گروه مهندسی مواد، دانشکده فنی و مهندسی، واحد شاهرود، دانشگاه آزاد اسلامی، شاهرود، سمنان، ایران

چکیده

در این پژوهش، بررسی و تولید هیدروکسی‌آپاتیت از استخوان ماهی زرد به روش هیدروترمال در دو دمای 150 و 200 درجه سلسیوس با استفاده از مواد افزودنی آب و الکل انجام شد. برای بررسی ساختار فازی، شناسایی ترکیبات آلی پودر و ریخت­ شناسی ذرات، به ­ترتیب از آنالیز پراش پرتو ایکس (XRD)، طیف‌سنجی مادون‌قرمز (FTIR) و میکروسکوپ الکترونی روبشی (SEM) استفاده شد. نتایج XRD نشان داد که پیک‌های مربوط به هیدروکسی‌آپاتیت، در محدوده  برابر با 30 تا 40 درجه قرار دارند. باتوجه ‌به نتایج به‌دست‌آمده، مشخص شد که برای تشکیل ساختار هیدروکسی‌آپاتیت، به حداقل دمای 200 درجه سلسیوس با محلول افزودنی آب نیاز است. نتایج FTIR نیز نشان داد که پیک‌ cm-1 1032، مربوط به گروه شیمیایی  و پیک cm-1 560، مربوط به  است. درنتیجه، پودر هیدروکسی‌آپاتیت ( ) به‌دست‌آمده، می‌تواند در کارهای پزشکی مورد استفاده قرار گیرد.

کلیدواژه‌ها

موضوعات

عنوان مقاله [English]

Investigation of Hydroxyapatite Production from Yellow Fish Bones by Hydrothermal Method

نویسندگان [English]

  • Jalaladdin Hosseinzadeh 1
  • Sahebali Manafi 2

1 M. Sc., Faculty of Engineering, Shahrood Branch, Islamic Azad University, Shahrood, Semnan, Iran

2 Professor, Department of Materials Engineering, Faculty of Engineering, Shahrood Branch, Islamic Azad University, Shahrood, Semnan, Iran

چکیده [English]

In this study, hydroxyapatite was produced and produced from yellow fish bones by hydrothermal method at two temperatures of 150 and 200 °C using water and alcohol additives. X-ray diffraction (XRD) analysis, infrared spectroscopy (FTIR) and scanning electron microscopy (SEM) were used to study the fuzzy structure, identification of powder organic compounds and particle morphology, respectively. XRD results showed that the peaks related to hydroxyapatite are in the range . According to the obtained results, it was found that to form the structure of hydroxyapatite, a minimum temperature of 200 degrees Celsius with water additive solution is required. The FTIR results also showed that the peak of 1032 cm-1 belongs to the chemical group and the peak of 560 cm-1 belongs to . As a result, the obtained hydroxyapatite powder ( ) can be used in medical work.

کلیدواژه‌ها [English]

  • Hydroxyapatite
  • Fish Bone
  • X-ray diffraction (XRD)
  • Infrared Spectroscopy (FTIR)
  • Scanning electron microscopy (SEM)
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