Journal of Advanced Materials and Technologies

Journal of Advanced Materials and Technologies

Investigation of Niobium Addition Effect on Oxidation Resistance of Ti-48Al/Ti2AlC Composite

Authors
Hadi Karimi
Ali Ghasemi
Morteza Hadi
Mohsen Sadeghi Mohammadi
Malek-Ashtar University of Technology, Department of Materials Engineering Shahin Shahr, Isfahan, Iran
10.30501/jamt.2636.70288
Abstract
In this research, the Ti-48Al/Ti2AlC and Ti-48Al(8Nb)/Ti2AlC composites were synthesized by means of
mechanical alloying and hot pressing. Firstly, the mixture of elemental powders were subjected to mechanical alloying
for 75 h and then to produce bulk samples, the milled powders were hot pressed for 1 h at 1000℃. Oxidation tests were
carried out in air at 1000 ℃ to compare the oxidation behavior of samples. Synthesized and oxidized samples were
studied by scanning electron microscopy, energy dispersive spectroscopy (EDS) and X-ray diffractometry (XRD).
According to X-ray diffraction patterns, the presence of γ-TiAl and Ti2AlC phases were detected for produced samples
and no phases on the base of Nb were formed. The results showed that the oxidation resistance of alloy was improved
by niobium addition. The growth of rutile was suppressed by substitution Nb for Ti in TiO2 lattice. Furthermore, scale
composition changed with addition of niobium that was related to the stabilization of nitride layer. 
Keywords
Ti-48Al/Ti2AlC composite
Mechanical alloying
Hot pressing
Oxidation
Niobium
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Journal of Advanced Materials and Technologies
Volume 4, Issue 1
Spring 2015
Pages 21-30

  • Receive Date 31 August 2014
  • Revise Date 15 March 2015
  • Accept Date 30 May 2015