Journal of Advanced Materials and Technologies

Journal of Advanced Materials and Technologies

Investigation of the Effect of Scan Speed and Laser Power on the Microstructure and Hardness Distribution of IN625 Deposited on a Gas Turbine Blade Using the LPBF Process

Document Type : Original Reaearch Article

Authors
1 Ph.D. Candidate, School of Metallurgy & Materials Engineering, Iran University of Science and Technology (IUST), Tehran, Iran.
2 Associate Professor , School of Metallurgy & Materials Engineering, Iran University of Science and Technology (IUST), Tehran, Iran.
3 Professor, School of Metallurgy & Materials Engineering, Iran University of Science and Technology (IUST), Tehran, Iran.
4 Professor, Metallurgy Research Department, Niroo Research Institute (NRI), Tehran, Iran.
5 Assistant Professor, Department of Ceramic, Materials and Energy Research Center, Karaj, Iran.
6 MSc, MAPNA Group, TUGA, Tehran, Iran
Abstract
Gas turbine components are predominantly manufactured from nickel-based superalloys. Operating under harsh conditions, these parts suffer from edge wear and reduced efficiency. Given the high cost of replacement, research into the cladding, refurbishment, and reusability of damaged components is of significant importance. While most existing studies have focused on Direct Energy Deposition (DED) techniques for cladding, Laser Powder Bed Fusion (LPBF) has received less attention. This study investigates the deposition of IN625 on a non-weldable IN738 substrate using LPBF, emphasizing its advantages over DED. The mechanisms of defect formation during manufacturing, along with their evaluation and control methods, are examined. To mitigate substrate-related defects, solution annealing and homogenization heat treatments were applied. To control defects in the deposited layer, process parameters such as scan speed and laser power were varied. Microhardness, as an indicator of mechanical performance at the cladded edges, was measured. The results revealed that microhardness is influenced not only by elemental concentration gradients but also by the cooling rate and the resulting cellular structure size. Consequently, an existing model from the literature, which correlates microhardness with elemental composition, was reassessed and modified. It was found that in dissimilar material joints, within a certain energy range, hardness becomes independent of composition and is instead governed by cell size. While the existing model from the literature fails to capture this behavior, the modified equation proposed in this study accurately predicts microhardness under such conditions.
Keywords

Subjects


  1. Adegoke, O., Andersson, J., Brodin, H., & Pederson, R. (2020). Influence of Laser Powder Bed Fusion Process Parameters on Voids, Cracks, and Microhardness of Nickel-Based Superalloy Alloy 247LC. Materials (Basel), 13(17), 3770. https://doi.org/10.3390/ma13173770
  2. Ahsan, F., & Ladani, L. (2020). Temperature profile, bead geometry, and elemental evaporation in laser powder bed fusion additive manufacturing process. Jom, 72(1), 429-439. https:/doi.org/10.1007/s11837-019-03872-3
  3. Badrossamay, M., Rezaei, A., Foroozmehr, E., Maleki, A., & Foroozmehr, A. (2022). Effects of increasing powder layer thickness on the microstructure, mechanical properties, and failure mechanism of IN718 superalloy fabricated by laser powder bed fusion. The International Journal of Advanced Manufacturing Technology, 1-15. https:/doi.org/10.1007/s00170-021-07719-7
  4. Basak, A., Acharya, R., & Das, S. (2016). Additive manufacturing of single-crystal superalloy CMSX-4 through scanning laser epitaxy: computational modeling, experimental process development, and process parameter optimization. Metallurgical and Materials Transactions A, 47(8), 3845-3859. https:/doi.org/10.1007/s11661-016-3571-y
  5. Benoit, M. J., Mazur, M., Easton, M. A., & Brandt, M. (2021). Effect of alloy composition and laser powder bed fusion parameters on the defect formation and mechanical properties of Inconel 625. The International Journal of Advanced Manufacturing Technology, 114, 915-927. https:/doi.org/10.1007/s00170-021-06957-z
  6. Bi, G., & Gasser, A. (2011). Restoration of nickel-base turbine blade knife-edges with controlled laser aided additive manufacturing. Physics Procedia, 12, 402-409. https:/doi.org/10.1016/j.phpro.2011.03.051
  7. Bian, L., Shamsaei, N., & Usher, J. M. (2017). Laser-based additive manufacturing of metal parts: modeling, optimization, and control of mechanical properties. CRC Press. https:/doi.org/10.1201/9781315151441
  8. Bridges, A., & Shingledecker, J. (2025). Creep Deformation and Damage Mechanisms in an Advanced High-Temperature Additively Manufactured Nickel-Base Superalloy. Jom, 1-22. https:/doi.org/10.1007/s11837-025-07326-x
  9. Cao, Y., Farouk, N., Taheri, M., Yumashev, A. V., Bozorg, S. F. K., & Ojo, O. O. (2021). Evolution of solidification and microstructure in laser-clad IN625 superalloy powder on GTD-111 superalloy. Surface and Coatings Technology, 412, 127010. https:/doi.org/10.1016/j.surfcoat.2021.127010
  10. Carter, L. N., Attallah, M. M., & Reed, R. C. (2012). Laser powder bed fabrication of nickel-base superalloys: influence of parameters; characterisation, quantification and mitigation of cracking. Superalloys, 2012(6), 2826-2834. https://doi.org/10.1002/9781118516430.ch64
  11. Carter, L. N., Martin, C., Withers, P. J., & Attallah, M. M. (2014). The influence of the laser scan strategy on grain structure and cracking behaviour in SLM powder-bed fabricated nickel superalloy. Journal of Alloys and Compounds, 615, 338-347. https:/doi.org/10.1016/j.jallcom.2014.06.172
  12. Caruso, M., & Frame, L. (2024). Ductility dip cracking mechanisms and characterization: a review. Journal of Materials Science, 59(36), 16789-16814. https:/doi.org/10.1007/s10853-024-10112-w
  13. Chauvet, E., Kontis, P., Jägle, E. A., Gault, B., Raabe, D., Tassin, C., Blandin, J.-J., Dendievel, R., Vayre, B., & Abed, S. (2018). Hot cracking mechanism affecting a non-weldable Ni-based superalloy produced by selective electron Beam Melting. Acta Materialia, 142, 82-94. https:/doi.org/10.1016/j.actamat.2017.09.047
  14. Danis, Y., Lacoste, E., & Arvieu, C. (2010). Numerical modeling of inconel 738LC deposition welding: Prediction of residual stress induced cracking. Journal of Materials Processing Technology, 210(14), 2053-2061. https:/doi.org/10.1016/j.jmatprotec.2010.07.027
  15. Dastgerdi, H. Z., Habib Shabani, A., Shajari Yazdan, Y., & Samiei. (2021). Effect of cooling rate on complete dissolution and aging time on microstructure and hardness of IN718 superalloy produced by selective laser melting (SLM). Journal of Advanced Materials and Technologies (JAMT), 10(2), 1-11. [In Persian] https://doi.org/10.30501/jamt.2020.224723.1080
  16. DebRoy, T., Wei, H. L., Zuback, J. S., Mukherjee, T., Elmer, J. W., Milewski, J. O., Beese, A. M., Wilson-Heid, A. d., De, A., & Zhang, W. (2018). Additive manufacturing of metallic components–process, structure and properties. Progress in Materials Science, 92, 112-224. https:/doi.org/10.1016/j.pmatsci.2017.10.001
  17. Donachie, M. J., & Donachie, S. J. (2002). Superalloys: a technical guide. ASM international. https:/doi.org/10.31399/asm.tb.stg2.9781627082679
  18. Fan, H., Shi, Q., Wang, C., Tian, Y., Zhou, K., & Yang, S. (2023). Laser powder bed fusion of bimetallic stainless steel/Nickel-based superalloy: Interface and mechanical properties. Materials Science and Engineering: A, 877, 145193. https:/doi.org/10.1016/j.msea.2023.145193
  19. Feng, K., Chen, Y., Deng, P., Li, Y., Zhao, H., Lu, F., Li, R., Huang, J., & Li, Z. (2017). Improved high-temperature hardness and wear resistance of Inconel 625 coatings fabricated by laser cladding. Journal of Materials Processing Technology, 243, 82-91. https:/doi.org/10.1016/j.jmatprotec.2016.12.001
  20. Gao, J., Chen, X., Yilmaz, O., & Gindy, N. (2008). An integrated adaptive repair solution for complex aerospace components through geometry reconstruction. The International Journal of Advanced Manufacturing Technology, 36, 1170-1179. https:/doi.org/10.1007/s00170-006-0923-6
  21. Haines, M. P., Rielli, V. V., Primig, S., & Haghdadi, N. (2022). Powder bed fusion additive manufacturing of Ni-based superalloys: a review of the main microstructural constituents and characterization techniques. Journal of Materials Science, 57(30), 14135-14187. https:/doi.org/10.1007/s10853-022-07501-4
  22. Henderson, M., Arrell, D., Larsson, R., Heobel, M., & Marchant, G. (2004). Nickel based superalloy welding practices for industrial gas turbine applications. Science and technology of welding and joining, 9(1), 13-21. https://doi.org/10.1179/136217104225017099
  23. Hisazawa, H., Terada, Y., Adziman, F., Crudden, D. J., Collins, D. M., Armstrong, D. E., & Reed, R. C. (2017). The effect of Nb/Ti ratio on hardness in high-strength Ni-based superalloys. Metals, 7(3), 71. https:/doi.org/10.3390/met7030071
  24. Hojjatzadeh, S. M. H., Parab, N. D., Yan, W., Guo, Q., Xiong, L., Zhao, C., Qu, M., Escano, L. I., Xiao, X., & Fezzaa, K. (2019). Pore elimination mechanisms during 3D printing of metals. Nature communications, 10(1), 1-8. https:/doi.org/10.1038/s41467-019-10973-9
  25. Huynh, T., Mehta, A., Graydon, K., Woo, J., Park, S., Hyer, H., Zhou, L., Imholte, D. D., Woolstenhulme, N. E., & Wachs, D. M. (2022). Microstructural development in Inconel 718 nickel-based superalloy additively manufactured by laser powder bed fusion. Metallography, Microstructure, and Analysis, 1-20. https:/doi.org/10.1007/s13632-021-00811-0
  26. Jiang, R., Mostafaei, A., Wu, Z., Choi, A., Guan, P. W., Chmielus, M., & Rollett, A. D. (2020). Effect of heat treatment on microstructural evolution and hardness homogeneity in laser powder bed fusion of alloy 718. Additive Manufacturing, 35, 101282. https:/doi.org/10.1016/j.addma.2020.101282
  27. Kang, H. S., Gwak, M., Kim, B. J., Park, K., Son, Y., Seo, S. M., Kim, S., Lee, H., & Kim, J. G. (2024). Repairing weld for directly solidified Ni-based superalloy substrates using directed energy deposition of Inconel 625. Materials Science and Engineering: A, 913, 147083. https:/doi.org/10.1016/j.msea.2024.147083
  28. Keshavarz, M. K., Turenne, S., & Bonakdar, A. (2018). Solidification behavior of inconel 713LC gas turbine blades during electron beam welding. Journal of Manufacturing Processes, 31, 232-239. https:/doi.org/10.1016/j.jmapro.2017.11.021
  29. Khodabakhshi, A., Mashreghi, A., Shajari, Y., & Razavi, S. H. (2018). Investigation of microstructure properties and quantitative metallography by different etchants in the service-exposed nickel-based superalloy turbine blade. Transactions of the Indian Institute of Metals, 71(4), 849-859. https:/doi.org/10.1007/s12666-017-1217-4
  30. Kreitcberg, A., & Brailovski, V. (2022). Effect of Fe and C contents on the microstructure and high-temperature mechanical properties of IN625 alloy processed by laser powder bed fusion. Materials, 15(19), 6606. https:/doi.org/10.3390/ma15196606
  31. Mohammadpour, P., Yuan, H., Li, Z., & Phillion, A. (2024). Evaluation of microstructure heterogeneity in INCONEL 625 thin-wall fabricated by Laser Powder Bed Fusion additive manufacturing. Materialia, 35, 102126. https:/doi.org/10.1016/j.mtla.2024.102126
  32. Montero-Sistiaga, M. L., Pourbabak, S., Van Humbeeck, J., Schryvers, D., & Vanmeensel, K. (2019). Microstructure and mechanical properties of Hastelloy X produced by HP-SLM (high power selective laser melting). Materials & Design, 165, 107598. https:/doi.org/10.1016/j.matdes.2019.107598
  33. Mostafaei, A., Ghiaasiaan, R., Ho, I.-T., Strayer, S., Chang, K.-C., Shamsaei, N., Shao, S., Paul, S., Yeh, A.-C., & Tin, S. (2023). Additive Manufacturing of Nickel-based superalloys: a state-of-the-art review on process-structure-defect-property relationship. Progress in Materials Science, 101108. https:/doi.org/10.1016/j.pmatsci.2023.101108
  34. Osoba, L., & Amuda, M. (2014). Tracking heat-affected zone cracking susceptibility in standard and modified heat treated IN 738 superalloy welds. High Performance and Optimum Design of Structures and Materials, 137, 37. http:/dx.doi.org/10.2495/HPSM140041
  35. Pohl, P. M., Kümmel, F., Schunk, C., Serrano-Munoz, I., Markötter, H., Göken, M., & Höppel, H. W. (2021). About the role of interfaces on the fatigue crack propagation in laminated metallic composites. Materials, 14(10), 2564. https://doi.org/10.3390/ma14102564
  36. Qi, T., Zhu, H., Zhang, H., Yin, J., Ke, L., & Zeng, X. (2017). Selective laser melting of Al7050 powder: Melting mode transition and comparison of the characteristics between the keyhole and conduction mode. Materials & Design, 135, 257-266. https:/doi.org/10.1016/j.matdes.2017.09.014
  37. Ramakrishnan, A., & Dinda, G. (2019). Direct laser metal deposition of Inconel 738. Materials Science and Engineering: A, 740, 1-13. https:/doi.org/10.1016/j.msea.2018.10.020
  38. Riazi, A., Razavi, S. H., Khavandi, A., Amirjan, M., Shabani, M. O., & Davarzani, H. (2024). A New Approach to the Reasons for Dependency of Defects Formation to the Process Parameters in Laser Powder Bed Fusion of IN625 on the IN738LC Substrate. Journal of Advanced Joining Processes, 100273. https:/doi.org/10.1016/j.jajp.2024.100273
  39. Riazi, A., Razavi, S. H., Khavandi, A., Amirjan, M., Shabani, M. O., & Davarzani, H. (2025). Influence of Process Parameters on Melt Pool Morphology and Elemental Diffusion in LPBF of IN625 on IN738 Substrate. Results in Surfaces and Interfaces, 100553. https:/doi.org/10.1016/j.rsurfi.2025.100553
  40. Rodenkirchen, C., Ackerman, A., Mignanelli, P., Cliff, A., Wise, G., Breul, P., Douglas, J., Bagot, P., Moody, M., & Appleton, M. (2023). Effect of alloying on the microstructure, phase stability, hardness, and partitioning behavior of a new dual-superlattice nickel-based superalloy. Metallurgical and Materials Transactions A, 54(5), 1902-1923. https:/doi.org/10.1007/s11661-023-06972-7
  41. Rottwinkel, B., Nölke, C., Kaierle, S., & Wesling, V. (2014). Crack repair of single crystal turbine blades using laser cladding technology. Procedia Cirp, 22, 263-267. https://doi.org/10.1016/j.procir.2014.06.151
  42. Shajari, Y., Razavi, S. H., Seyedraoufi, Z. S., & Samiee, M. (2021). The effect of time and temperature of solutionizing heat treatment on γ′ characterization in a Ni-base superalloy. Metallography, Microstructure, and Analysis, 10(4), 441-447. https:/doi.org/10.1007/s13632-021-00760-8
  43. Soffel, F., Lin, Y., Keller, D., Egorov, S., & Wegener, K. (2021). Laser remelting process simulation and optimization for additive manufacturing of Nickel-based super alloys. Materials, 15(1), 177. https://doi.org/10.3390/ma15010177
  44. Thompson, S. M., Bian, L., Shamsaei, N., & Yadollahi, A. (2015). An overview of Direct Laser Deposition for additive manufacturing; Part I: Transport phenomena, modeling and diagnostics. Additive Manufacturing, 8, 36-62. https:/doi.org/10.1016/j.addma.2015.07.001
  45. Tucho, W. M., Cuvillier, P., Sjolyst-Kverneland, A., & Hansen, V. (2017). Microstructure and hardness studies of Inconel 718 manufactured by selective laser melting before and after solution heat treatment. Materials Science and Engineering: A, 689, 220-232. https:/doi.org/10.1016/j.msea.2017.02.062
  46. Ur Rehman, A., Pitir, F., & Salamci, M. U. (2021). Laser powder bed fusion (LPBF) of In718 and the impact of pre-heating at 500 and 1000°C: Operando Study. Materials, 14(21), 6683. https:/doi.org/10.3390/ma14216683
  47. Weng, T. S., & Tsai, C. H. (2014). Laser-induced backside wet cleaning technique for glass substrates. Applied Physics A, 116, 597-604. https:/doi.org/10.1007/s00339-013-8182-5
  48. Xu, J., Ding, Y., Gao, Y., Wang, H., Hu, Y., & Zhang, D. (2021). Grain refinement and crack inhibition of hard-to-weld Inconel 738 alloy by altering the scanning strategy during selective laser melting. Materials & Design, 209, 109940. https:/doi.org/10.1016/j.matdes.2021.109940
  49. Yang, H., Yang, J., Huang, W., Wang, Z., & Zeng, X. (2018). The printability, microstructure, crystallographic features and microhardness of selective laser melted Inconel 718 thin wall. Materials & Design, 156, 407-418. https:/doi.org/10.1016/j.matdes.2018.07.007
  50. Yeung, H., Kim, F., Donmez, M., & Neira, J. (2022). Keyhole pores reduction in laser powder bed fusion additive manufacturing of nickel alloy 625. International Journal of Machine Tools and Manufacture, 183, 103957. https:/doi.org/10.1016/j.ijmachtools.2022.103957
  51. Zhou, Z., Sun, W., Wu, J., Chen, H., Zhang, F., & Wang, S. (2023). The fundamental mechanisms of laser cleaning technology and its typical applications in industry. Processes, 11(5), 1445. https:/doi.org/10.3390/pr11051445
Volume 14, Issue 1
Spring 2025
Pages 43-61

  • Receive Date 13 April 2025
  • Revise Date 22 April 2025
  • Accept Date 21 May 2025